DBU-promoted Cu(OAc)<subscript>2</subscript>·H<subscript>2</subscript>O-catalysed coupling reactions of aryl iodides and sodium azide.
In: Journal of Chemical Research, Jg. 42 (2018-06-01), Heft 5, S. 247-250
Online
academicJournal
Zugriff:
An efficient and simple protocol for the synthesis of aryl azides by the coupling of aryl iodides with sodium azide, in good to excellent yields in DMSO at 95 °C under catalysis by Cu(OAc)2·H2O and 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU), has been established. The optimised loadings of Cu(OAc)2·H2O and DBU were 10 mol% and 15 mol% respectively. [ABSTRACT FROM AUTHOR]
Titel: |
DBU-promoted Cu(OAc)<subscript>2</subscript>·H<subscript>2</subscript>O-catalysed coupling reactions of aryl iodides and sodium azide.
|
---|---|
Autor/in / Beteiligte Person: | Jiang, Yuqin ; Suo, Huajun ; Zhao, Yaru ; Li, Xiyong ; Sun, Yamin ; Li, Xingfeng ; Dong, Wenpei ; Li, Wei ; Zhang, Weiwei ; Xu, Guiqing |
Link: | |
Zeitschrift: | Journal of Chemical Research, Jg. 42 (2018-06-01), Heft 5, S. 247-250 |
Veröffentlichung: | 2018 |
Medientyp: | academicJournal |
ISSN: | 1747-5198 (print) |
DOI: | 10.3184/174751918X15260507766192 |
Schlagwort: |
|
Sonstiges: |
|