SYNTHESIS, PHYSICO-CHEMICAL CHARACTERIZATION, AND ANTIBACTERIAL STUDIES OF SOME BIOACTIVE SCHIFF BASES AND THEIR METAL CHELATES
In: Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, Jg. 32 (2002-09-26), S. 1485-1500
Online
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Zugriff:
Complexes of Co(II), Ni(II) and Cu(II) with the Schiff bases salicylidene–2- aminophenol (H2SAPh), furfurylidene-N-phenylthiourea (FNPTU) and salicylidene-N-phenylthiourea (HSNPTU) have been synthesized and their physico-chemical properties have been investigated with the help of microanalytical data, UV-Vis, IR, ESR speotroscopy, TGA, conductance and magnetic susceptibility measurements. Non-isothermal kinetic and ligand field parameters of some complexes have been calculated. The general formula of the salicylidene-2-aminophenol Co(II) and Ni(II) complexes is [ML(H2O)3]·2H2O and for the Cu(II) complex It is [CuL(H2O)]·H2O. The Furfurylidene-N-phenylthiourea and salicylidene-N-phenylthiourea complexes are of the general formulae [ML2Cl2]·2H2O and [ML2]·2H2O. These complexes have also been screened for their antibacterial properties and a few of them have been tested against tubercular bacteria.
Titel: |
SYNTHESIS, PHYSICO-CHEMICAL CHARACTERIZATION, AND ANTIBACTERIAL STUDIES OF SOME BIOACTIVE SCHIFF BASES AND THEIR METAL CHELATES
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Autor/in / Beteiligte Person: | Khare, Mahima ; Mishra, A. P. ; Gautam, S. K. |
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Zeitschrift: | Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, Jg. 32 (2002-09-26), S. 1485-1500 |
Veröffentlichung: | Informa UK Limited, 2002 |
Medientyp: | unknown |
ISSN: | 1532-2440 (print) ; 0094-5714 (print) |
DOI: | 10.1081/sim-120014864 |
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