Synthesis and Spectroscopic Studies of some Divalent Metall Ion Complexes of 3-(4-hydroxyphenyl)-2-(3-(4-nitrobenzoyl) thioureido) propanoic acid
In: Baghdad Science Journal, Jg. 14 (2017), Heft 3, S. 588-596
Online
academicJournal
Zugriff:
3-(4-hydroxyphenyl)-2-(3-(4-nitrobenzoyl) thioureido) propanoic acid (HNP) a new ligand was synthesized by reaction of Tyrosine with (4-Nitrobenzoyl isothiocyanate) by using acetone as a solvent. The prepared ligand (HNP) has been characterized by elemental analysis (CHNS), infrared (FT-IR), electronic spectral (Ultraviolet visible) and(1H,13C-Nuclear Magnetic Resonance) spectra. Some Divalent metal ion complexes of (HNP) were prepared and spectroscopic studies by Fourier transform infrared (FTIR), electronic spectral(UV-Vis), molar conductance, magnetic susceptibility and atomic absorption. The results measured showed the formula of six prepared complexes were [M (HNP)2] (M+2 = Manganese, Cobalt, Nickel, Znic, Cadmium and Mercury),from the obtained data tetrahedral structure suggested for all complexes, except Copper complex has a square planer geometry
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Synthesis and Spectroscopic Studies of some Divalent Metall Ion Complexes of 3-(4-hydroxyphenyl)-2-(3-(4-nitrobenzoyl) thioureido) propanoic acid
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Autor/in / Beteiligte Person: | Sarhan, Basima M. ; Neema, Ban Z. |
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Zeitschrift: | Baghdad Science Journal, Jg. 14 (2017), Heft 3, S. 588-596 |
Veröffentlichung: | College of Science for Women, University of Baghdad, 2017 |
Medientyp: | academicJournal |
ISSN: | 2078-8665 (print) ; 2411-7986 (print) |
DOI: | 10.21123/bsj.2017.14.3.0588 |
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