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Homogeneous alumoxane-LCT-epoxy polymers and methods for making the same

Smith, James D.B.
2005
Online Patent

Titel:
Homogeneous alumoxane-LCT-epoxy polymers and methods for making the same
Autor/in / Beteiligte Person: Smith, James D.B.
Link:
Veröffentlichung: 2005
Medientyp: Patent
Sonstiges:
  • Nachgewiesen in: USPTO Patent Applications
  • Sprachen: English
  • Document Number: 20050009958
  • Publication Date: January 13, 2005
  • Appl. No: 10/618111
  • Application Filed: July 11, 2003
  • Claim: 1. A method of making homogeneous alumoxane-LCT-epoxy polymers with a dielectric strength of at least 1.2 kV/mil comprising: mixing at least one LCT-epoxy resin with at least one boehmite material, under sufficient conditions to form a uniform dispersion and an essentially complete co-reactivity of said at least one boehmite material with said at least one LCT-epoxy resin, wherein a mixture is formed; and curing said mixture to produce said homogeneous alumoxane-LCT-epoxy polymers; wherein the amount of said at least one boehmite material to said at least one LCT-epoxy resin comprises a ratio of between 3:17 and 13:7 by weight.
  • Claim: 2. The method of claim 1, wherein said at least one boehmite material comprises carboxylate-alumoxane.
  • Claim: 3. The method of claim 2, wherein said carboxylate-alumoxane is 4-hydroxybenoate-alumoxane.
  • Claim: 4. The method of claim 1, wherein the alumoxane portions of said homogeneous alumoxane-LCT-epoxy polymers is 20-50% by weight.
  • Claim: 5. The method of claim 1, wherein mixing said at least one LCT-epoxy resin with said at least one boehmite material comprises first pre-heating said at least one LCT-epoxy resin until said at least one LCT-epoxy resin is clear.
  • Claim: 6. The method of claim 1, wherein mixing said at least one LCT-epoxy resin and said at least one boehmite material further comprises warming until said mixture is clear.
  • Claim: 7. The method of claim 1, further comprising mixing at least one anhydriding agent with at least one of said at least one LCT-epoxy resin and said boehmite material, wherein said homogeneous alumoxane-LCT-epoxy polymers are a homogeneous alumoxane-LCT-epoxy-anhydride polymers.
  • Claim: 8. The method of claim 7, wherein said anhydriding agent is taken from the group consisting of 1-methylhexahydrophthalic anhydride and 1-methyltetrahydrophthalic anhydride.
  • Claim: 9. The method of claim 7, wherein said anhydriding agent is approximately 25-45% by weight of said homogeneous alumoxane-LCT-epoxy-anhydride polymers.
  • Claim: 10. The method of claim 1, wherein curing of said mixture comprises adding one of the group consisting of zinc naphthenate and chromium acetylacetonate.
  • Claim: 11. The method of claim 1, wherein said mixture is added to an electrical insulator as a coating before curing.
  • Claim: 12. A method of making homogeneous alumoxane-LCT-epoxy polymers with a dielectric strength of at least 1.2 kV/mil coated on at least one electrical insulator comprising the steps of: mixing at least one LCT-epoxy resin with at least one boehmite material, wherein a mixture is formed; warming until said mixture is clear and under sufficient conditions to form a uniform dispersion and an essentially complete co-reactivity of said at least one boehmite material with said at least one LCT-epoxy resin; impregnating said mixture onto said electrical insulator; and curing said mixture to produce said homogeneous alumoxane-LCT-epoxy polymers; wherein the amount of said at least one boehmite material to said at least one LCT-epoxy resin comprises a ratio of between 3:17 and 13:7 by weight.
  • Claim: 13. The method of making homogeneous alumoxane-LCT-epoxy polymers coated on at least one electrical insulator as in claim 12, further comprising adding to said at least one LCT-epoxy resin at least one anhydriding agent prior to adding said boehmite material, wherein said homogeneous alumoxane-LCT-epoxy polymers are homogeneous alumoxane-LCT-epoxy-anhydride polymers.
  • Claim: 14. The method of making homogeneous alumoxane-LCT-epoxy polymers coated on at least one electrical insulator as in claim 12, wherein said electrical insulator is a mica/glass insulating tape.
  • Claim: 15. Homogeneous alumoxane-LCT-epoxy polymers comprising: at least one alumoxane containing sub-structure; at least one LCT-epoxy sub-structure; thermal conductivity in the transverse direction of at least 0.50 W/mK and in the thickness direction of at least 0.99 W/mK in an environment of 25° C.; and dielectric strength of at least 1.2 kV/mil; wherein said alumoxane substructure is organically bonded to said LCT-epoxy substructure; wherein approximately 15-65% by weight of said homogeneous alumoxane-LCT-epoxy polymers is said alumoxane sub-structure; and wherein said homogeneous alumoxane-LCT-epoxy polymers are substantially free of particle wetting and micro-void formation.
  • Claim: 16. The homogeneous alumoxane-LCT-epoxy polymers of claim 15, wherein said alumoxane sub-structure comprises carboxylate-alumoxane.
  • Claim: 17. The homogeneous alumoxane-LCT-epoxy polymers of claim 16, wherein said carboxylate-alumoxane is 4-hydroxybenoate-alumoxane
  • Claim: 18. The homogeneous alumoxane-LCT-epoxy polymers of claim 15, wherein said homogeneous alumoxane-LCT-epoxy polymers contain at least one anhydride, and wherein said anhydride portion is approximately 25-45% by weight of said homogeneous alumoxane-LCT-epoxy polymers.
  • Claim: 19. The homogeneous alumoxane-LCT-epoxy polymers of claim 15, wherein said homogeneous alumoxane-LCT-epoxy polymers are integrally formed with at least one electrical insulator.
  • Current U.S. Class: 523457/000

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